反应条件
in hexane
byproducts: H2, CO; (Ar); for 15 min; evapd., extd. (hexane), ext. concd., crystd. at -40°C fractionally, mother liquor concd., chromd. (SiO2), concd., crystd. at -40°C overnight, crystals sepd. manually, recrystd. at -4°C; obtainedanal. impure;
参考文献
Ghosh; Lei; Shang; Fehlner
Inorganic Chemistry, 2000 , vol. 39, # 23 p. 5373 - 5382