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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
15226-74-1
合成路线
（共 158 条）
15226-74-1
+
75-04-7
乙胺
→
反应条件
7403-41-0
4-甲氧基-N-乙基苯甲酰胺
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
15226-74-1
+
78-81-9
异丁胺
→
反应条件
7464-51-9
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
15226-74-1
+
100-46-9
苄胺
→
反应条件
7465-87-4
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
110-91-8
吗啉
+
104-92-7
4-溴苯甲醚
+
15226-74-1
→
反应条件
7504-58-7
吗啉基(4-甲氧基苯基)甲酮
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
110-91-8
吗啉
+
15226-74-1
+
696-62-8
4-碘苯甲醚
→
反应条件
7504-58-7
吗啉基(4-甲氧基苯基)甲酮
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
15226-74-1
→
反应条件
7608-17-5
苯基乙炔基二苯基膦
反应条件
in dichloromethane under N2, stirring, 8 h; evapn.; recrystn. (CH2Cl2/CH3OH);
参考文献
Louattani, Elmostafa; Suades, Joan; Mathieu, Rene
Journal of Organometallic Chemistry, 1991 , vol. 421, # 2-3 p. 335 - 340
764-93-2
1-癸炔
+
15226-74-1
→
反应条件
1235569-13-7
+
73317-94-9
+
7694-77-1
+
87969-80-0
反应条件
1: 1-n-decyne; dicobalt octacarbonyl; N,N,N'-trimethyl-N'-allylthiourea With 1,1,3,3-tetramethyl-2-thiourea in toluene Pauson-Khand reaction; 0.0833333 h; Inert atmosphere; 2: carbon monoxide in toluene T=110°C; Pauson-Khand reaction; P=2250.23 Torr; 22 h; Autoclave;
参考文献
Petrovski, Zeljko; Martins, Bruno M.R.; Afonso, Carlos A.M.
Tetrahedron Letters, 2010 , vol. 51, # 26 p. 3356 - 3359
15226-74-1
+
2780-89-4
→
反应条件
6621-60-9
反应条件
triethylamine in acetonitrile T=100°C; 0.75 h; Inert atmosphereMicrowave irradiation;
参考文献
Fontan, Noelia; Garcia-Dominguez, Patricia; Alvarez, Rosana; De Lera, Angel R.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 7 p. 2056 - 2067
15226-74-1
+
107-11-9
→
反应条件
66897-25-4
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=90°C; 0.333333 h; Sealed tubeMicrowave irradiation;
参考文献
Baburajan, Poongavanam; Elango, Kuppanagounder P.
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1006 - 1010
764-93-2
1-癸炔
+
15226-74-1
→
反应条件
1235569-13-7
+
73317-94-9
+
7694-77-1
+
87969-80-0
反应条件
1: 1-n-decyne; dicobalt octacarbonyl; N,N,N'-trimethyl-N'-allylthiourea With 1,1,3,3-tetramethyl-2-thiourea in toluene Pauson-Khand reaction; 0.0833333 h; Inert atmosphere; 2: carbon monoxide in toluene T=110°C; Pauson-Khand reaction; P=2250.23 Torr; 22 h; Autoclave;
参考文献
Petrovski, Zeljko; Martins, Bruno M.R.; Afonso, Carlos A.M.
Tetrahedron Letters, 2010 , vol. 51, # 26 p. 3356 - 3359
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