2,2-二甲基-5-苯基-1,3-二氧杂环乙烷-4,6-二酮合成路线 (共 12 条)
反应条件
1: 68 percent / K2CO3 / dimethylformamide
2: 67 percent / Sc(OTf)3 / nitromethane / 1 h / 100 °C
View Scheme
参考文献
Fillion, Eric; Fishlock, Dan; Wilsily, Ashraf; Goll, Julie M.
Journal of Organic Chemistry, 2005 , vol. 70, # 4 p. 1316 - 1327
反应条件
acetic anhydride in ethylene glycol dimethyl ether
Ambient temperature;
参考文献
Jacobs, Robert T.; Wright, Allen D.; Smith, Francis X.
Journal of Organic Chemistry, 1982 , vol. 47, # 19 p. 3769 - 3772