4,4,4-三氟-3-羟基-1-苯基丁烷-1-酮合成路线 （共 23 条）
反应条件
hydrogen; Pt/Al2O3 in toluene T=24°C; P=7500.6 Torr; 2 h;
参考文献
Hess, Reto; Diezi, Simon; Mallat, Tamas; Baiker, Alfons
Tetrahedron Asymmetry, 2004 , vol. 15, # 2 p. 251 - 257
反应条件
in hexane 1 h; Ambient temperature;
参考文献
Funabiki, Kazumasa; Matsunaga, Kei; Nojiri, Miwa; Hashimoto, Wataru; Yamamoto, Hitoshi; Shibata, Katsuyoshi; Matsui, Masaki
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2853 - 2860
反应条件
in hexane 1 h; Ambient temperature;
参考文献
Funabiki, Kazumasa; Matsunaga, Kei; Nojiri, Miwa; Hashimoto, Wataru; Yamamoto, Hitoshi; Shibata, Katsuyoshi; Matsui, Masaki
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2853 - 2860
参考文献
Showa Shell Sekiyu Kabushiki Kaisha
Patent: US4929760 A1, 1990 ;
反应条件
in various solvent(s) Heating;
参考文献
Funabiki, Kazumasa; Matsunaga, Kei; Nojiri, Miwa; Hashimoto, Wataru; Yamamoto, Hitoshi; Shibata, Katsuyoshi; Matsui, Masaki
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2853 - 2860
反应条件
1: in hexane Substitution; 1 h; Heating; 2: With silica gel in hexane; ethyl acetate Deamination;
参考文献
Funabiki, Kazumasa; Matsunaga, Kei; Nojiri, Miwa; Hashimoto, Wataru; Yamamoto, Hitoshi; Shibata, Katsuyoshi; Matsui, Masaki
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2853 - 2860
反应条件
1: in hexane Substitution; 1 h; Heating; 2: With silica gel in hexane; ethyl acetate Deamination;
参考文献
Funabiki, Kazumasa; Matsunaga, Kei; Nojiri, Miwa; Hashimoto, Wataru; Yamamoto, Hitoshi; Shibata, Katsuyoshi; Matsui, Masaki
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2853 - 2860
反应条件
zinc(II) iodide in 1,4-dioxane
参考文献
Kubota, Toshio; Iijima, Masahiro; Tanaka, Tatsuo
Tetrahedron Letters, 1992 , vol. 33, # 10 p. 1351 - 1354
反应条件
1: in hexane Substitution; 1 h; Heating; 2: With silica gel in hexane; ethyl acetate Deamination;
参考文献
Funabiki, Kazumasa; Matsunaga, Kei; Nojiri, Miwa; Hashimoto, Wataru; Yamamoto, Hitoshi; Shibata, Katsuyoshi; Matsui, Masaki
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2853 - 2860
反应条件
in tetrahydrofuran T=-78°C; 4 h; Inert atmosphere;
参考文献
Marrec, Olivier; Borrini, Julien; Billard, Thierry; Langlois, Bernard R.
Synlett, 2009 , # 8 p. 1241 - 1244
