反应条件
1: 85 percent / n-BuLi / diethyl ether / 1.5 h / -78 °C 2: 1.) DIBAL-H, 2.) N-bromosuccimide / 1.) hexane, RT, 20 h, 2.) hexane, from -20 deg C to RT, 3 h 3: 1.) n-BuLi, 2.) red Se / 1.) diethyl ether, reflux, 2 h, 2.) diethyl ether, from 0 deg C to RT View Scheme
参考文献
Kurita; Ishii; Yasuike; Tsuchiya
Chemical and Pharmaceutical Bulletin, 1994 , vol. 42, # 7 p. 1437 - 1441
