5-硝基-6-甲氧基(1H)吲唑合成路线 （共 7 条）
反应条件
1: With acetic anhydride; potassium carbonate in chloroform; acetic acid T=40°C; 2: With isopentylnitrile in chloroform; acetic acid T=60°C; 3: With hydrogenchloride in methanol T=80°C; 2 h;
参考文献
US2012/15962 A1, ;
Page/Page column 89-90 ;
US 20120015962 A1
反应条件
sodium nitrate; sulfuric acid in water T=20°C;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 12, # 9 p. 2115 - 2137
反应条件
1.1: potassium acetate / CHCl3 / 20 - 40 °C 1.2: isoamyl nitrite / CHCl3 / 60 °C 2.1: HCl / methanol / 80 °C 3.1: sodium nitrate; H2SO4 / H2O / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 12, # 9 p. 2115 - 2137
反应条件
1: HCl / methanol / 80 °C 2: sodium nitrate; H2SO4 / H2O / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 12, # 9 p. 2115 - 2137
反应条件
1.1: nitric acid; sulfuric acid / acetic acid / 3 h / 5 - 10 °C 2.1: potassium carbonate; acetic anhydride / chloroform; acetic acid / 40 °C 2.2: 60 °C 2.3: 2 h / 80 °C View Scheme
参考文献
US2012/15962 A1, ;
US 20120015962 A1
反应条件
acetic acid Diazotization;
参考文献
Journal of the Chemical Society, , p. 2412,2419
参考文献
Arora, Nidhi; Chen, Shaoqing; Hermann, Johannes Cornelius; Kuglstatter, Adreas; Labadie, Sharada Shenvi; Lin, Clara Jeou Jen; Lucas, Matthew C.; Moore, Amy Geraldine; Papp, Eva; Talamas, Francisco Xavier; Wanner, Jutta; Zhai, Yansheng
Patent: US2012/15962 A1, 2012 ;
Location in patent: Page/Page column 90 ;
US 20120015962 A1
