乙基(5-bromo-2-nitropyridin-3-yl)氨基甲酸酯合成路线 （共 2 条）
反应条件
1: 82 percent / K2CO3 / acetone / 6 h / Heating 2: 75 percent / aq. KOH / ethanol / 1 h / Heating 3: 61 percent / (PPh3)4Pd, NaCO3 / benzene; ethanol / 2 h / Heating 4: 1.) H2 / Raney Ni / 1.) RT, 1 atm, 2.) 200 deg C, 3 h View Scheme
参考文献
Linstroem, Stefan; Eriksson, Mikael; Grivas, Spiros
Acta Chemica Scandinavica, 1993 , vol. 47, # 8 p. 805 - 812
反应条件
water; potassium hydroxide in tetrahydrofuran
T=90°C;
参考文献
van Duzer, John H.; Mazitschek, Ralph
Patent: US2014/128391 A1, 2014 ;
Location in patent: Paragraph 0226; 0231; 0232 ;
