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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
152714-07-3
合成路线
（共 9 条）
152714-04-0
→
反应条件
152714-07-3
反应条件
hydrogen; sodium acetate; palladium on activated charcoal in methanol
参考文献
Wiberg, Kenneth B.; Shobe, David; Nelson, Gordon L.
Journal of the American Chemical Society, 1993 , vol. 115, # 23 p. 10645 - 10652
191019-76-8
→
反应条件
152714-07-3
反应条件
zinc in acetic acid 14 h; Ambient temperature;
参考文献
Resende, Patricia; Almeida, Wanda P.; Coelho, Fernando
Tetrahedron Asymmetry, 1999 , vol. 10, # 11 p. 2113 - 2118
1073-67-2
4-氯苯乙烯
→
反应条件
152714-07-3
反应条件
1: 91 percent / Zn-Cu; POCl3 / diethyl ether / 20 h / 20 °C 2: 93 percent / Zn; AcOH / 14 h / 20 °C View Scheme
参考文献
Wiberg, Kenneth B.; Shobe, David; Nelson, Gordon L.
Journal of the American Chemical Society, 1993 , vol. 115, # 23 p. 10645 - 10652
152714-00-6
→
反应条件
152714-07-3
反应条件
1: 77 percent / conc. H2SO4 / 0.28 h / Heating 2: 85 percent / AcONa, H2 / Pd/C / methanol View Scheme
参考文献
Wiberg, Kenneth B.; Shobe, David; Nelson, Gordon L.
Journal of the American Chemical Society, 1993 , vol. 115, # 23 p. 10645 - 10652
152713-97-8
→
反应条件
152714-07-3
反应条件
1: KOH / aq. ethanol / 21 h / Ambient temperature 2: 77 percent / conc. H2SO4 / 0.28 h / Heating 3: 85 percent / AcONa, H2 / Pd/C / methanol View Scheme
参考文献
Wiberg, Kenneth B.; Shobe, David; Nelson, Gordon L.
Journal of the American Chemical Society, 1993 , vol. 115, # 23 p. 10645 - 10652
1073-67-2
4-氯苯乙烯
+
76-02-8
三氯乙酰氯
→
反应条件
152714-07-3
反应条件
zinc; trichlorophosphate 1.) Et2O, reflux; 2.) AcOH, reflux; Yield given. Multistep reaction;
参考文献
Mazzini, Claudio; Lebreton, Jacques; Alphand, Veronique; Furstoss, Roland
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1195 - 1196
152714-07-3
→
反应条件
22518-27-0
4-(4-氯苯基)-2-吡咯烷酮
反应条件
formic acid; hydroxylamine-o-sulphonic acid 10 h; Heating;
参考文献
Coelho, Fernando; De Azevedo, Mariangela B. M.; Boschiero, Roberta; Resende, Patricia
Synthetic Communications, 1997 , vol. 27, # 14 p. 2455 - 2465
152714-07-3
→
反应条件
69308-37-8
(R)-巴氯芬
反应条件
1.1: 70 percent / lithium (S,S')-α,α'-dimethylbenzamide / tetrahydrofuran; hexane / 0.17 h / -100 °C 2.1: O3 / CH2Cl2; methanol / 0.67 h / -78 °C 2.2: Me2S / CH2Cl2; methanol / 12 h / -78 - 20 °C 2.3: NaBH3CN; AcONH4 / methanol / 12 h / 20 °C View Scheme
参考文献
Resende, Patricia; Almeida, Wanda P.; Coelho, Fernando
Tetrahedron Asymmetry, 1999 , vol. 10, # 11 p. 2113 - 2118
152714-07-3
→
反应条件
63701-55-3
R(+)-巴氯芬盐酸盐
反应条件
1: oxidation by culture of the bacteria Acinetobacter calcoaceticus NCIMB 9871 2: 95 percent / Me3SiI / CH2Cl2 / 0 deg C to r.t. 3: 95 percent / NaN3 / dimethylformamide / 75 °C 4: 95 percent / 1.) NaOH (2M); 2.) conc.HCl / Ambient temperature 5: 80 percent / 1.) H2; 2.) HCl gas / 1.) Pd-C / diethyl ether; ethanol / 760 Torr / Ambient temperature View Scheme
参考文献
Mazzini, Claudio; Lebreton, Jacques; Alphand, Veronique; Furstoss, Roland
Tetrahedron Letters, 1997 , vol. 38, # 7 p. 1195 - 1196
