methylamine; HCl in water amine and Pt-compound kept at 50°C overnight; filtration; excess of amine evapd. (water-bath); addn. of concd. HCl; heating on water-bath for 1 h; elem. anal.;
in neat (no solvent)
byproducts: NH(CH3)2; thermal decompn. of Pt-complex at 555-615 K; further by-products;
参考文献
Al Takhin, Ghassan; Skinner, Henry A.; Zaki, Ahmed A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 2323 - 2328
