反应条件
in ethanol; water under N2, covered by Al foil, PMe3 was distd. in chlorauric acid dissolved in H2O-EtOH cooled to -35°C, stirred for 2.5 h at -20°C; modified from Duddell, D. A., Goggin, P. L., Goodfellow, R. J. et al., J. Chem. Soc. A, 1970, 545; filtered, recrystd. from acetone-MeOH;
参考文献
Bruce, Michael I.; Horn, Ernst; Matisons, Janis G.; Snow, Michael R.
Australian Journal of Chemistry, 1984 , vol. 37, # 6 p. 1163 - 1170
