反应条件
n-butyllithium in diethyl ether; hexane
Ar atmosphere; cooling soln. of n-BuLi in hexane and Et2O (-70°C), addn. of Sn-compd. (ratio n-BuLi/Sn-compd. 3:1), stirring (60 min, -70°C), warming (room temp., 60 min), quenching with Me3GeCl, stirring (15 min); hydrolysation (aq. NH4Cl), diln. (Et2O), sepn. of org. layer, washing (H2O), drying (MgSO4), evapn.; elem. anal.;
参考文献
Boer, Henricus J. R. de; Akkerman, Otto S.; Bickelhaupt, Fridrich
Organometallics, 1990 , vol. 9, p. 2898 - 2903
