反应条件
in tetrahydrofuran
byproducts: CH3SCH2MgCH3; under anaerobic conditions, in NMR tube; Sn compd., Mg compd. (molar ratio 1:1) in THF, SnMe4 (internal standard) and THF mixed; reacted for 12 d; not isolated; monitored by (119)Sn NMR spectra; 10percent conversion;
参考文献
Yousef, Rushdi I; Rueffer, Tobias; Schmidt, Harry; Steinborn, Dirk
Journal of Organometallic Chemistry, 2002 , vol. 655, # 1-2 p. 111 - 114
