in neat (no solvent) byproducts: C2H5Br; addn. of Br2 to Sn-compound with stirring for 1.5 h at 70°C, boiling under reflux for 3.5 h at 90-100°C; distn. (vac.), elem. anal.;
参考文献
Medvedev, S. V.; Yatsenko, A. V.
Journal of General Chemistry USSR (English Translation), 1986 , vol. 56, p. 1912 - 1912
Zhurnal Obshchei Khimii, 1986 , vol. 56, p. 2166 - 2166
Br2 in tetrachloromethane Br2 soln. (CCl4) addn. to Sn-compds. soln. (butyl bromide) at room temp.; alkyl halide excess removal (transcondn. into trap in liq. nitrogen); gas chromy.;
参考文献
Pomeshchikov, V. D.; Pozdeev, V. V.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 2283 - 2287
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 2583 - 2588
Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.5.4.5, page 106 - 108
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Fentiman, A. F.; Wyant, R. E.; Steinmeyer, R. D.; Jeffrey, D. A.; Kircher, J. F.; Kahler, E. J.
BMI-1613 (1965) 14 S.
