反应条件
1.1: sodium iodate; sulfuric acid / 2 h / 110 °C
1.2: 70 percent / sodium iodide; copper(I) iodide / dimethylformamide / 5 h / 110 °C
2.1: 57 percent / pyridine / 8 h / 95 °C
3.1: 72 percent / tin(II) chloride dihydrate / ethanol; ethyl acetate / 4 h / 85 °C
4.1: sodium nitrite; hydrochloric acid / acetonitrile; H2O / 0.5 h / 0 °C
4.2: 14 percent / potassium iodide / acetonitrile; H2O / 18 h / 20 °C
5.1: 86 percent / n-butyllithium / tetrahydrofuran; hexane / -78 - -42 °C
View Scheme
参考文献
Lee, Chung-Chieh; Leung, Man-Kit; Lee, Gene-Hsiang; Liu, Yi-Hung; Peng, Shie-Ming
Journal of Organic Chemistry, 2006 , vol. 71, # 22 p. 8417 - 8423
