1-二乙基氨基-3-(苯氧基)丙-2-醇合成路线 (共 6 条)
反应条件
lithium perchlorate in diethyl ether
T=20°C; 0.5 h;
参考文献
Heydari, Akbar; Mehrdad, Morteza; Maleki, Aziz; Ahmadi, Nafiseh
Synthesis, 2004 , # 10 p. 1563 - 1565
反应条件
1.1: (CF3)3COH / chiral polymer-supported Co(salen) complex / 6 h / 4 - 25 °C
1.2: KOH / diethyl ether / 3 h / 25 °C
2.1: Yb(OTf)3 / CH2Cl2 / 16 h / 25 °C
View Scheme
参考文献
Peukert, Stefan; Jacobsen, Eric N.
Organic Letters, 1999 , vol. 1, # 8 p. 1245 - 1248
反应条件
ytterbium(III) triflate in dichloromethane
T=25°C; 16 h;
参考文献
Peukert, Stefan; Jacobsen, Eric N.
Organic Letters, 1999 , vol. 1, # 8 p. 1245 - 1248
反应条件
hydrogenchloride in diethyl ether
T=0°C;
参考文献
Papini, Annamaria; Ricci, Alfredo; Taddei, Maurizio; Seconi, Giancarlo; Dembech, Pasquale
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2261 - 2266
参考文献
Geartner,V.R.
Journal of Organic Chemistry, 1968 , vol. 33, # 2 p. 523 - 530
反应条件
potassium hydroxide
1.) RT, 36 h, 2.) ethanol, reflux, 4 h; Yield givenMultistep reaction;
参考文献
Sharma; Talwar; Gupta, Anu
Journal of the Indian Chemical Society, 1997 , vol. 74, # 4 p. 343 - 344