O-(三甲基硅烷基)苯酚合成路线 （共 28 条）
反应条件
1: pyridine / 3 h / Ambient temperature 2: 92 percent Chromat. / NaI, NCS / acetic acid / 1 h / 60 °C View Scheme
参考文献
Wilbur, D. S.; Stone, W. E.; Anderson, K. W.
Journal of Organic Chemistry, 1983 , vol. 48, # 9 p. 1542 - 1544
反应条件
18-crown-6 ether; nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile T=60°C; 2 h; Inert atmosphere;
参考文献
Ikawa, Takashi; Nishiyama, Tsuyoshi; Nosaki, Toshifumi; Takagi, Akira; Akai, Shuji
Organic Letters, 2011 , vol. 13, # 7 p. 1730 - 1733
反应条件
pyridine in dichloromethane T=0°C; Inert atmosphere;
参考文献
Atkinson, Darcy J.; Sperry, Jonathan; Brimble, Margaret A.
Synthesis, 2010 , # 6 p. 911 - 913
反应条件
in acetonitrile T=23°C; 2.33333 h; Inert atmosphere;
参考文献
Bronner, Sarah M.; Garg, Neil K.
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8842 - 8843
反应条件
1: triethylamine; 4-pyrrolidin-1-ylpyridine / tetrahydrofuran; hexane / 0.06 h / 55 °C / |Flow reactor 2: tetrakis(triphenylphosphine) palladium(0); cesium fluoride / acetonitrile / 16 h / 55 °C / |Microwave irradiation View Scheme
参考文献
Michel, Boris; Greaney, Michael F.
Organic Letters, 2014 , vol. 16, # 10 p. 2684 - 2687
参考文献
Sasaki, Tadashi; Usuki, Arimitsu; Ohno, Masatomi
Journal of Organic Chemistry, 1980 , vol. 45, # 18 p. 3559 - 3564
反应条件
N-chloro-succinimide; sodium bromide in methanol 0.0833333 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 48, # 9 p. 1542 - 1544
反应条件
in not given at 250°C;;
参考文献
Gilman, H.; Nobis, J. F.
Journal of the American Chemical Society, 1950 , vol. 72, p. 2629 - 2632
Full Text View citing articles Show Details
Speier, J. L.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1003 - 1010
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Gmelin Handbook: Si: MVol.C, 22, page 68 - 71
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Dow Corning Corp.
Patent: US2611777 , 1952 ;
C. A., 1953 , p. 4127
反应条件
bromine in N,N-dimethyl-formamide
参考文献
EASTMAN KODAK COMPANY
Patent: EP601643 A2, 1994 ;
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=20°C; Inert atmosphere;
参考文献
Atkinson, Darcy J.; Sperry, Jonathan; Brimble, Margaret A.
Synthesis, 2010 , # 6 p. 911 - 913
