according to R. L. Dannley, G. C. Farrant, G. C. J. Org. Chem. 34 (1969)2428;
参考文献
Thomas, John Meurig; Sankar, Gopinathan; Klunduk, Marek C.; Attfield, Martin P.; Maschmeyer, Thomas; Johnson, Brian F. G.; Bell, Robert G.
Journal of Physical Chemistry B, 1999 , vol. 103, # 42 p. 8809 - 8813
MgSO4 in benzene to soln. germanol in benzene MgSO4 was added and stirred at reflux temp.for 12 h; solvent was removed in vacuo, product was purified by GPLC;
参考文献
Goto, Kei; Shimo, Isao; Kawashima, Takayuki
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 12 p. 2389 - 2394
→
反应条件
in benzene byproducts: tert.-butyl alcohol; Ti compd. added with stirring to Ph3GeOH in benzene; mixt. stored at room temp. for 24 h; filtered;
参考文献
Stepovik; Gulenova
Russian Journal of General Chemistry, 2006 , vol. 76, # 2 p. 235 - 244
