反应条件
CCl4 in toluene Kinetics; At 70-90°C 7-germabenzonorbornadiene-compound is added to CCl4, filled under argon into the NMR tube, and heated in a thermostat for 3 h, thermal decompn.,; GC analysis demonstrates the presence of C2Cl6 and Me2GeCl2 in yields of 100 percent and 95 percent, Me2ClGeCCl3 is detected by (1)H NMR, tetraphenylnaphthalene is pptd. with EtOH (quant. yield);
参考文献
Organometallics, , vol. 7, p. 1201 - 1207
