反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in hexane N2-atmosphere; stirring and refluxing thiophene with BuLi and TMEDA for 2 h, add. of excess Me2GeCl2, stirring at room temp. for 3 h; collection (filtration), washing (water, MeOH, hexane), drying (vac.); elem. anal.;
参考文献
Barrau; Rima; Akkari; Satge
Inorganica Chimica Acta, 1997 , vol. 260, # 1 p. 11 - 15
