2: 99 percent / lithium tert-butyl hydroperoxide / tetrahydrofuran; toluene / 0.5 h / -78 °C
3: 69 percent / lithium iodide / acetone / 1 h / Heating
4: 67 percent / magnesium iodide / diethyl ether / 288 h / Ambient temperature
View Scheme
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3091 - 3102
Jackson, Richard F. W.; Standen, Stephen P.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 2 p. 149 - 156
2: 92 percent / lithium tert-butyl hydroperoxide / tetrahydrofuran; toluene / a) -78 deg C, 10 min, b) -18 deg C, 55 min
3: 3 percent / lithium iodide / acetone / 1 h / Heating
View Scheme
参考文献
Hewkin, Cheryl T.; Jackson, Richard F. W.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3091 - 3102
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=-20°C; 3 h;
参考文献
Jackson, Richard F. W.; Standen, Stephen P.; Clegg, William
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 2 p. 149 - 156
