4-氯苄基三苯基氯化磷蓊盐合成路线 （共 13 条）
反应条件
in xylene 18 h; Heating;
参考文献
Warner, Philip; Sutherland, Robert
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6294 - 6300
反应条件
1: SOCl2 / toluene / 0.08 h / Ambient temperature 2: xylene / 22 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 42, # 6 p. 1007 - 1017
反应条件
1: LAH 2: conc. aq. HCl / 12 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 21 p. 5643 - 5649
反应条件
hydrogenchloride 12 h; Heating; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 21 p. 5643 - 5649
反应条件
1: 1.) n-BuLi / 1.) toluene, hexane, 15 min, 2.) toluene, hexane, 3 h 2: 74 percent / KMnO4, aq. MgSO4 / toluene / 40 h / 50 - 60 °C View Scheme
参考文献
Aitken, R. Alan; Cadogan, J. I. G.; Gosney, Ian
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 101, # 1-4 p. 281 - 286
反应条件
potassium tert-butylate; iodine 1) EtOH, 1 h, 2) toluene, reflux; Yield given. Multistep reaction;
参考文献
Warner, Philip; Sutherland, Robert
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6294 - 6300
反应条件
1: 18-crown-6 ether; potassium carbonate / dichloromethane; water / 24 h / 20 °C 2: 24 h / 250 °C View Scheme
参考文献
Ho, Jinn-Hsuan; Lin, Yu-Chen; Chou, Li-Ting; Chen, Ying-Zhe; Liu, Wei-Qi; Chuang, Chao-Li
Tetrahedron Letters, 2013 , vol. 54, # 15 p. 1991 - 1993
反应条件
1: (i) NaNH2, liq. NH3, Fe(NO3)3, (ii) /BRN= 386303/, benzene 2: aq. ethanol / (electrolysis) View Scheme
参考文献
Bestmann,H.-J. et al.
Justus Liebigs Annalen der Chemie, 1967 , vol. 704, p. 109 - 141
反应条件
1: 1.) n-BuLi / 1.) toluene, hexane, 15 min, 2.) toluene, hexane, 3 h
2: 62 percent / KMnO4, aq. MgSO4 / toluene / 50 h / 50 - 60 °C
View Scheme
参考文献
Aitken, R. Alan; Cadogan, J. I. G.; Gosney, Ian
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 101, # 1-4 p. 281 - 286
反应条件
sodium ethanolate in ethanol; toluene
Heating;
参考文献
Briquet, Anne Andree Sophie; Hansen, Hans-Juergen
Helvetica Chimica Acta, 1994 , vol. 77, p. 1921 - 1939
