1,4-二(癸基氧基)-2,5-二碘苯合成路线 （共 5 条）
反应条件
1: 69 percent / K2CO3 / acetone / 3 h / Heating 2: 41 percent / KIO3; I2; acetic acid / H2SO4 / H2O / 11 h / Heating View Scheme
参考文献
Shirai, Yasuhiro; Zhao, Yuming; Cheng, Long; Tour, James M.
Organic Letters, 2004 , vol. 6, # 13 p. 2129 - 2132
Title/Abstract Full Text View citing articles Show Details
Zhao, Yuming; Shirai, Yasuhiro; Slepkov, Aaron D.; Cheng, Long; Alemany, Lawrence B.; Sasaki, Takashi; Hegmann, Frank A.; Tour, James M.
Chemistry - A European Journal, 2005 , vol. 11, # 12 p. 3643 - 3658
反应条件
1: 80 percent / KOH / ethanol / Heating 2: 83 percent / I2; Hg(OAc)2 / CH2Cl2 / 20 °C View Scheme
参考文献
Shirai, Yasuhiro; Zhao, Yuming; Cheng, Long; Tour, James M.
Organic Letters, 2004 , vol. 6, # 13 p. 2129 - 2132
Title/Abstract Full Text View citing articles Show Details
Zhao, Yuming; Shirai, Yasuhiro; Slepkov, Aaron D.; Cheng, Long; Alemany, Lawrence B.; Sasaki, Takashi; Hegmann, Frank A.; Tour, James M.
Chemistry - A European Journal, 2005 , vol. 11, # 12 p. 3643 - 3658
反应条件
1: 69 percent / K2CO3 / acetone / 3 h / Heating 2: 41 percent / KIO3; I2; acetic acid / H2SO4 / H2O / 11 h / Heating View Scheme
参考文献
Plater, M. John; Sinclair, James P.; Aiken, Stuart; Gelbrich, Thomas; Hursthouse, Michael B.
Tetrahedron, 2004 , vol. 60, # 30 p. 6385 - 6394
反应条件
1: 89 percent / CuI; TEA / [PdCl2(PPh3)2] / tetrahydrofuran / 20 °C 2: 95 percent / K2CO3 / tetrahydrofuran; methanol / 4 h / 20 °C View Scheme
参考文献
Shirai, Yasuhiro; Zhao, Yuming; Cheng, Long; Tour, James M.
Organic Letters, 2004 , vol. 6, # 13 p. 2129 - 2132
反应条件
hydrogenchloride; tert.-butyl lithium in tetrahydrofuran react. of 8 equiv B(OMe)3 with mixt. C6H2(OC10H21)2I2 and t-BuLi (5 equiv), addn. HCl (1 M);
参考文献
Goldfinger, Marc B.; Swager, Timothy M.
Journal of the American Chemical Society, 1994 , vol. 116, # 17 p. 7895 - 7896
