N-(2,6-二氯苯基)-N-苯基-氯乙酰胺合成路线 （共 6 条）
反应条件
T=106 - 110°C; Acetylation; 2 h;
参考文献
Ryabova; Bokanov; Isakovich; Kuzovkin; Grigor'ev; Levina; Shvedov; Granik
Pharmaceutical Chemistry Journal, 1996 , vol. 30, # 1 p. 38 - 40
反应条件
1: 99 percent / TiCl4 / toluene / 2 h / 20 °C 2: Et3N / dimethylformamide / 5 h / 95 - 100 °C 3: 86 percent / 2 h / 106 - 110 °C View Scheme
参考文献
Pharmaceutical Chemistry Journal, , vol. 30, # 1 p. 38 - 40
反应条件
1: 99 percent / TiCl4 / toluene / 2 h / 20 °C 2: Et3N / dimethylformamide / 5 h / 95 - 100 °C 3: 86 percent / 2 h / 106 - 110 °C View Scheme
参考文献
Pharmaceutical Chemistry Journal, , vol. 30, # 1 p. 38 - 40
反应条件
1: Et3N / dimethylformamide / 5 h / 95 - 100 °C 2: 86 percent / 2 h / 106 - 110 °C View Scheme
参考文献
Pharmaceutical Chemistry Journal, , vol. 30, # 1 p. 38 - 40
反应条件
1: 75.4 percent / AlCl3 / 2 h / 160 °C 2: 93 percent / 2 N NaOH / ethanol; H2O / 4 h / Heating View Scheme
参考文献
Moser; Sallmann; Wiesenberg
Journal of Medicinal Chemistry, 1990 , vol. 33, # 9 p. 2358 - 2368
反应条件
aluminium trichloride T=160°C; 2 h;
参考文献
Moser; Sallmann; Wiesenberg
Journal of Medicinal Chemistry, 1990 , vol. 33, # 9 p. 2358 - 2368
