(2,5-二甲基-苯基磺酰基)-乙酸合成路线 （共 4 条）
反应条件
1: With potassium hydroxide in ethanol
18 h;
2: With ethanol; water
18 h;
3: With hydrogenchloride; water
T=4°C; pH=1; 18 h;
参考文献
EMISPHERE TECHNOLOGIES, INC.; WANG, Nai, Fang; SARAF, Sushma; PUSZTAY, Stephen, V.
Patent: WO2008/14430 A1, 2008 ;
Location in patent: Page/Page column 57 ;
反应条件
alkaline solution
T=70 - 80°C;
参考文献
Ciba
Patent: DE622938 , 1933 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 21, p. 990
Full Text Show Details
Ciba
Patent: US2017613 , 1933 ;
反应条件
1: benzene; zinc-powder; water / 60 - 70 °C
2: aqueous alkaline solution / 70 - 80 °C
View Scheme
参考文献
Ciba
Patent: DE622938 , 1933 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 21, p. 990
Full Text Show Details
Ciba
Patent: US2017613 , 1933 ;
反应条件
sulfuryl dichloride; antimony(V) pentachloride; chlorobenzene
T=30 - 60°C;
参考文献
Ciba
Patent: DE622938 , 1933 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 21, p. 990
Full Text Show Details
Ciba
Patent: US2017613 , 1933 ;
