反应条件
trimethylamine oxide dihydrate in acetonitrile byproducts: trimethylamine, CO2; soln. of Rh-complex and Me3NO*2H2O in CH3CN boiled under reflux (1 h), mixt. cooled, evapn. of solvent (vac.), addn. of Ph3P and isopropanol to oily residue, react. mass boiled (1 h); cryst. ppt. filtered, washed (1. EtOH, 2. Et2O), dried (air);
参考文献
Kukushkin, V. Yu.; Dushina, M. E.; Krylov, V. K.; Iretskii, A. V.
Sov. J. Coord. Chem. (Engl. Transl.), 1987 , vol. 13, p. 364 - 369
Koordinatsionnaya Khimiya, 1987 , vol. 13, p. 650 - 655