反应条件
in benzene stirring of Fe2(CO)9 with silane (24 h), addn. of further Fe2(CO)9 (total molar ratio Fe:Si=2.4:1), stirring (24 h); evapn. (vac., low temp.), dissoln. in hexane, filtration (Florisil), solvent removal, dissoln. in hexane, crystn. of Fe3(CO)12 (-30°C), evapn. of mother liquor; elem. anal.;
参考文献
Cundy, Colin S.; Lappert, Michael F.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 665 - 673
