反应条件
in diethyl ether Dropwise addn. of PhLi to Fe2(CO)9 (Et2O, -5°C, Ar, over 1 h), stirring (2 h), evapn., addn. of H2O and n-hexane, treating with Me3OBF4 with stirring.; Organic layer is separated, aq. layer is extd. (n-hexane), organic soln. is dried (Na2SO4, 1 h) and concd., chromy. (silica gel, n-hexane).;
参考文献
Organometallics, , vol. 7, p. 812 - 818
