in benzene soln. of ferrocenylcarbinol is degassed (N2) and refluxed for 15 h in presence of Fe2(CO)9; react. mixt. is filtered over Celite, concd. and chromatographed (silica gel 60, CH2Cl2/hexane), elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 379, p. 129 - 138
in benzene soln. of ferrocenylcarbinol is degassed (N2) and refluxed in presence of Fe2(CO)9 for 5 h; react. mixt. is filtered over Celite, concd. and chromatographed (silica gel 60, CH2Cl2/hexane);
参考文献
Journal of Organometallic Chemistry, , vol. 379, p. 129 - 138
in benzene a mixture of Fe2(CO)9, PH2p-tol and benzene was stirred under N2 for 10 h;; removal of solvent in vac.; extrn. with n-hexane; removal of solvent in vac.;
参考文献
De; Biswas
Journal of the Indian Chemical Society, 1991 , vol. 68, # 6 p. 347 - 348
in decalin Sonication; (Ar); products identified IR, UV, mass spect., chromy.;
参考文献
Dewar, J.; Jones, H. O.
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1907 , vol. 79, p. 74 - 74
octadecanoic acid in mineral oil heating of mixt. of mineral oil, Fe2(CO)9 and stearic acid at 573 K under Ar flow for 30 min; cooling at the velocity of 0.074 K/s to 314 K;
参考文献
Bica, Loan
Journal of Magnetism and Magnetic Materials, 2004 , vol. 283, # 2-3 p. 335 - 343
