反应条件
in benzene
N2-atmosphere; 3 equiv. of ligand, 8-10°C, 1-2 days (to beginningof formation of tricarbonyl-complex); filtration, evapn. (below 5°C), dissoln. in cold Et2O, cooling to-80°C (crystn. of excess ligand), filtration, evapn. of filtrate , dissoln. in pentane (-20°C), crystn. (below 0°C); elem. anal.;
参考文献
Drake,J.E.; Hemmings,R.T.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 1730 - 1734
