N-乙酰基-2-(4-氟苯基)-甘氨酸合成路线 (共 7 条)
反应条件
sulfuric acid; lithium bromide; [PdBr2(PPh3)2] in various solvent(s) T=120°C; P=45003.6 Torr; 12 h;
参考文献
Beller, Matthias; Eckert, Markus; Geissler, Holger; Napierski, Bernd; Rebenstock, Heinz-Peter; Holla, E. Wolfgang
Chemistry - A European Journal, 1998 , vol. 4, # 5 p. 935 - 941
反应条件
sodium hydrogencarbonate in water; acetone T=-5 - 20°C; 3 h;
参考文献
Soloshonok, V. A.; Galaev, I. Yu.; Shvyadas, V. K.; Kozlova, E. V.; Kotik, N. V.; et al.
Russian Journal of Bioorganic Chemistry, 1993 , vol. 19, # 4 p. 228 - 232
Bioorganicheskaya Khimiya, 1993 , vol. 19, # 4 p. 467 - 473
反应条件
sodium hydroxide in ethanol 0.5 h; Heating; Yield given;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 5 p. 613 - 619
反应条件
1: 1.) Pb(OAc)4, Hg(OAc)2, 2.) pyridine / 1.) CHCl3, 40 deg C, 1 h, 2.) 40 deg C, 1 h 2: aq. NaOH / ethanol / 0.5 h / Heating View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 5 p. 613 - 619
反应条件
sodium hydroxide 1.) CHCl3, pyridine; 2.) EtOH, H2O, reflux; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 35, # 51 p. 9625 - 9628
参考文献
Bulletin de la Societe Chimique de France, , vol. <II>, p. 248 - 254
反应条件
water aminoacylase from Streptoverticillium olivoreticuli;
参考文献
Russian Journal of Bioorganic Chemistry, , vol. 19, # 4 p. 228 - 232
Bioorganicheskaya Khimiya, , vol. 19, # 4 p. 467 - 473