甲基7-氮杂双环[2.2.1]庚-2-烯-7-羧酸酯合成路线 （共 6 条）
参考文献
Otten, Albert; Namyslo, Jan Christoph; Stoermer, Martin; Kaufmann, Dieter E.
European Journal of Organic Chemistry, 1998 , # 9 p. 1997 - 2001
反应条件
1: 99 percent / H2 / Pd/C / methanol 2: 39 percent / Na/Hg View Scheme
参考文献
Clayton, Simon C.; Regan, Andrew C.
Tetrahedron Letters, 1993 , vol. 34, # 46 p. 7493 - 7496
反应条件
1: 81 percent / CH2Cl2 / 9000720 Torr 2: 99 percent / H2 / Pd/C / methanol 3: 39 percent / Na/Hg View Scheme
参考文献
Clayton, Simon C.; Regan, Andrew C.
Tetrahedron Letters, 1993 , vol. 34, # 46 p. 7493 - 7496
反应条件
1: 99 percent / dipotassium azodicarboxylate, acetic acid / methanol; H2O / 0 - 20 °C 2: 86 percent / tetra-n-butylammonium fluoride trihydrate / tetrahydrofuran / 16 h / 20 °C View Scheme
参考文献
Otten, Albert; Namyslo, Jan Christoph; Stoermer, Martin; Kaufmann, Dieter E.
European Journal of Organic Chemistry, 1998 , # 9 p. 1997 - 2001
反应条件
sodium amalgam 1.) acetonitrile, 50 deg C, 12 kbar, 20 h; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Seerden, Jean-Paul G.; Tulp, Martin Th. M.; Scheeren, Hans W.; Kruse, Chris G.
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 11 p. 2103 - 2110
反应条件
1: trimethylamine / CHCl3 / 3.5 h / Heating
2: methanol / CH2Cl2 / 0.17 h / Heating
View Scheme
参考文献
Altenbach, Hans-Josef; Constant, Dieter; Martin, Hans-Dieter; Mayer, Bernhard; Mueller, Monika; Vogel, Emanuel
Chemische Berichte, 1991 , vol. 124, # 4 p. 791 - 801
