6-硝基-3,4-亚甲基二氧苄乙醇合成路线 （共 5 条）
反应条件
sodium tetrahydroborate; H16PcZn in PEG-400 T=20°C; 1.5 h;
参考文献
Sharma, Upendra; Kumar, Neeraj; Verma, Praveen Kumar; Kumar, Vishal; Singh, Bikram
Green Chemistry, 2012 , vol. 14, # 8 p. 2289 - 2293
反应条件
nitric acid; acetic acid T=-10 - 0°C; 0.25 h; Inert atmosphere;
参考文献
Tietze, Lutz F.; Mueller, Michael; Duefert, Svenia-C.; Schmuck, Kianga; Schuberth, Ingrid
Chemistry - A European Journal, 2013 , vol. 19, # 5 p. 1726 - 1731
反应条件
1: 96 percent / Et3N; SOCl2 / CH2Cl2 / 3 h / 0 - 20 °C 2: 5 percent / dimethylsulfoxide / 120 h / 20 °C / Irradiation View Scheme
参考文献
Meuche-Albeny; Rathelot; Crozet; Vanelle
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 8 p. 989 - 997
反应条件
thionyl chloride; triethylamine in dichloromethane T=0 - 20°C; 3 h;
参考文献
Meuche-Albeny; Rathelot; Crozet; Vanelle
Chemistry of Heterocyclic Compounds, 2003 , vol. 39, # 8 p. 989 - 997
参考文献
Carter et al.
Journal of Pharmacy and Pharmacology, 1958 , vol. 10, p. Spl. 149 T, 153 T
