1,3-苯并噁唑-2-乙腈合成路线 （共 7 条）
反应条件
Al3+ exchanged K10 clay in anhydrous xylene T=140°C; 16 h; Green chemistry;
参考文献
Suresh, Dhanusu; Dhakshinamoorthy, Amarajothi; Pitchumani, Kasi
Tetrahedron Letters, 2013 , vol. 54, # 48 p. 6415 - 6419
反应条件
1: in acetic acid; glacial; ethanol T=100°C; 24 h; Heating / reflux; 2: With sodium hydrogencarbonate in dichloromethane; water
参考文献
KINETEK PHARMACEUTICALS, INC.
Patent: WO2004/11460 A2, 2004 ;
Location in patent: Page 61-62 ;
WO 2004/011460 A2
反应条件
in N,N-dimethyl-formamide T=90°C;
参考文献
Ilkun, Olesya T.; Archibald, Stephen J.; Barnes, Charles L.; Gerasimchuk, Nikolay; Biagioni, Richard; Silchenko, Svitlana; Gerasimchuk, Olga A.; Nemykin, Victor N.
Dalton Transactions, 2008 , # 42 p. 5715 - 5729
反应条件
in toluene 3 h; Reflux;
参考文献
Rady, Eman A. El
Heterocyclic Communications, 2012 , vol. 18, # 4 p. 215 - 221
反应条件
ammonium acetate in ethanol
1 h; Heating;
参考文献
Elnagdi, M. H.; Abdallah, S. O.; Ghoneim, K. M.; Ebied, E. M.; Kassab, K. N.
Journal of Chemical Research, Miniprint, 1997 , # 2 p. 375 - 384
反应条件
1: With KPF6; {RuCl2(1-methyl-4-(1-methylethyl)benzene)}2
T=55°C; 19 h; Inert atmosphere;
2: With water in methanol
参考文献
Ben Ammar, Hamed; Miao, Xiaowei; Fischmeister, Cedric; Toupet, Loic; Dixneuf, Pierre H.
Organometallics, 2010 , vol. 29, # 19 p. 4234 - 4238
反应条件
1: 60 percent / ammonium acetate / ethanol / 1 h / Heating
2: 65 percent / pyridine / 0.08 h / 100 °C
View Scheme
参考文献
Elnagdi, M. H.; Abdallah, S. O.; Ghoneim, K. M.; Ebied, E. M.; Kassab, K. N.
Journal of Chemical Research, Miniprint, 1997 , # 2 p. 375 - 384
