反应条件
1: 50 percent / 1.) LiN(SiMe3)2; 2.) MoOPH (Vedjes' molybdenum peroxide) / 1.) THF, -78 deg C, 1.5 h; 2.) - 78 deg C, 6 h
2: NaBH4 / methanol / 0 °C
3: NEt3 / CH2Cl2 / 0 - 25 °C
4: 70 percent / (NH4)2Ce(NO3)6 / acetonitrile; H2O / 0 °C
View Scheme
参考文献
Palomo; Aizpurua; Miranda; Mielgo; Odriozola
Tetrahedron Letters, 1993 , vol. 34, # 39 p. 6325 - 6328
