反应条件
1: 4-chlorophenyl phosphorodichloridate / pyridine / 0 - 5 deg C, 2 h; RT, overnight
2: aq. NH3; dioxane / 2 h / Ambient temperature
3: 85 percent / tetra-n-butylammonium fluoride / tetrahydrofuran / 0.5 h / Ambient temperature
View Scheme
参考文献
Lin, Tai-Shun; Luo, Mei-Zhen; Liu, Mao-Chin
Tetrahedron, 1995 , vol. 51, # 4 p. 1055 - 1068