(2S,3R)-3-methyl-2-phenyl-3,4-dihydro-2H-benzo[4,5]thiazolo[3,2-a]pyrimidine; sodium sulfate; N-ethyl-N,N-diisopropylamine in toluene T=-40°C; 11 h; Resolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Zhang, Yuhua; Birman, Vladimir B.
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 14-15 p. 2525 - 2529
Na-Pi buffer; tubers of Solanum tuberosum cv. Saturna in acetone 48 h; other racemic alcohols, pH 5.9, other biologically active material: tubers of Helianthus tuberosus; Product distribution;
Na-Pi buffer; tubers of Solanum tuberosum cv. Saturna in acetone 48 h; other racemic alcohols, pH 5.9, other biologically active material: tubers of Helianthus tuberosus; Product distribution;
oxygen; anhydrous cobalt diacetate; ozone in ethyl acetate T=20°C; 1.5 h; Yield givenYields of byproduct given. Title compound not separated from byproducts;
参考文献
Odinokov; Botsman; Emel'yanova
Russian Chemical Bulletin, 1998 , vol. 47, # 10 p. 2021 - 2022