1,2-二(1-萘基)乙烷合成路线 (共 82 条)
反应条件
magnesium in tetrahydrofuran T=20°C; 2.5 h; Reflux;
参考文献
Okamoto, Hideki; Yamaji, Minoru; Gohda, Shin; Kubozono, Yoshihiro; Komura, Noriko; Sato, Kaori; Sugino, Hisako; Satake, Kyosuke
Organic Letters, 2011 , vol. 13, # 10 p. 2758 - 2761
反应条件
oxygen in cyclohexane T=24.9°C; P=760 Torr;
参考文献
Barcus, R. L.; Hadel, L. M.; Johnston, L. J.; Platz, M. S.; Savino, T. G.; Scaiano, J. C.
Journal of the American Chemical Society, 1986 , vol. 108, # 14 p. 3928 - 3937
反应条件
methyl-magnesium iodide; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in benzene T=46°C; 18 h;
参考文献
Wang, Maw Cherng; Luh, Tien-Yau
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2178 - 2182
反应条件
Ti(III)-citrate; Tris buffer; tetra(n-butyl)ammonium hydroxide; B12 in ethanol pH=8; 1 h;
参考文献
Aitken, R. Alan; Hodgson, Philip K.G.; Morrison, John J.; Oyewale, Adebayo O.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 3 p. 402 - 415
反应条件
iodine; magnesium in tetrahydrofuran T=30°C; 3 h; SonicationInert atmosphere;
参考文献
Gozhina, Olga V.; Thomassen, Ivar K.; Lejon, Tore
Synthetic Communications, 2013 , vol. 43, # 14 p. 1867 - 1870
反应条件
methyl-magnesium iodide; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in benzene T=46°C; 18 h;
参考文献
Wang, Maw Cherng; Luh, Tien-Yau
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2178 - 2182
反应条件
mercury(I) fluoride in acetonitrile T=20°C; Decarboxylation; dimerization; Irradiation;
参考文献
Habibi, Mohammad H.; Farhadi, Saeid
Tetrahedron Letters, 1999 , vol. 40, # 14 p. 2821 - 2824
反应条件
in 2,2,4-trimethylpentane 2 h; Ambient temperatureIrradiation;
参考文献
Griffin, G. William; Horn, Keith A.
Journal of the American Chemical Society, 1987 , vol. 109, # 16 p. 4919 - 4926
反应条件
1: 96 percent / NaOEt / ethanol / 3 h / Heating 2: 81 percent / 30percent H2O2 / acetic acid; acetic anhydride / 48 h / -5 °C 3: benzene / 10 h / Irradiation View Scheme
参考文献
Wang, Maw Cherng; Luh, Tien-Yau
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2178 - 2182
反应条件
1: Et3N 2: 660 °C View Scheme
参考文献
Givens,R.S. et al.
Journal of the American Chemical Society, 1974 , vol. 96, # 17 p. 5547 - 5552