1,2-二(1-萘基)乙烷合成路线 (共 82 条)
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in benzene T=46°C; 18 h; other thioethers;
参考文献
Wang, Maw Cherng; Luh, Tien-Yau
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2178 - 2182
反应条件
in diethyl ether T=-100 - 25°C;
参考文献
Yang, Lau S.; Engler, Thomas A.; Shechter, Harold
Journal of the Chemical Society, Chemical Communications, 1983 , # 16 p. 866 - 868
反应条件
methanol Ambient temperatureIrradiation;
参考文献
Slocum, Gregory H.; Kaufmann, Kenneth; Schuster, Gary B.
Journal of the American Chemical Society, 1981 , vol. 103, # 15 p. 4625 - 4627
反应条件
sodium lauryl sulfate in acetonitrile T=-30.1°C; Irradiationsenzitizer: none, acetophenone; micellization; effect of external magnetic field; cage effect; temperature dependence of triplet decay parameters; ΔH(excit.); MechanismProduct distributionKinetics;
参考文献
Gould; Tung; Turro; Givens; Matuszewski
Journal of the American Chemical Society, 1984 , vol. 106, # 6 p. 1789 - 1793
反应条件
W(CO)6 in chlorobenzene 48 h; Heating; Further byproducts given;
参考文献
Ng, Chi Tat; Wang, Xiaojun; Luh, Tien-Yau
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2536 - 2539
反应条件
in acetonitrile 10 h; Ambient temperatureIrradiation;
参考文献
Koshima, Hideko; Ding, Kuiling; Chisaka, Yosuke; Matsuura, Teruo; Miyahara, Ikuko; Hirotsu, Ken
Journal of the American Chemical Society, 1997 , vol. 119, # 43 p. 10317 - 10324
反应条件
in benzene 10 h; Irradiation; Further byproducts given;
参考文献
Givens, Richard S.; Hrinczenko, Borys; Liu, Jerry H.-S.; Matuszewski, Bogdan; Tholen-Collison, Joan
Journal of the American Chemical Society, 1984 , vol. 106, # 6 p. 1779 - 1789
反应条件
in benzene 1 h; Ambient temperatureIrradiation;
参考文献
Koshima, Hideko; Ding, Kuiling; Chisaka, Yosuke; Matsuura, Teruo; Miyahara, Ikuko; Hirotsu, Ken
Journal of the American Chemical Society, 1997 , vol. 119, # 43 p. 10317 - 10324
反应条件
iodine; magnesium in tetrahydrofuran T=30°C; 3 h; SonicationInert atmosphere; Overall yield = 82 percent;
参考文献
Gozhina, Olga V.; Thomassen, Ivar K.; Lejon, Tore
Synthetic Communications, 2013 , vol. 43, # 14 p. 1867 - 1870
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iron(II) oxalate dihydrate T=155 - 160°C; 0.833333 h; Product distribution; Further Variations:Reagentstime;
参考文献
Khurana, Jitender M.; Chauhan, Sushma; Maikap, Golak C.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 10 p. 1737 - 1740