雄甾-1,4,9(11)-三烯-3,17-二酮合成路线 （共 5 条）
参考文献
Robinson et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2195,2197, 2198
反应条件
toluene-4-sulfonic acid in tetrahydrofuran T=20°C;
参考文献
Zhang, Bei Na; Chen, Ying; Zhang, Qian; Xia, Peng
Steroids, 2007 , vol. 72, # 1 p. 60 - 63
反应条件
72 h; Rhizopus stolonifer ATCC 6227b; Product distribution;
参考文献
Holland, Herbert L.; Riemland, Elly
Canadian Journal of Chemistry, 1985 , vol. 63, p. 1121 - 1126
反应条件
1: 92.1 percent / Si(0); KF / ethane-1,2-diol; various solvent(s) / 2 h / 140 °C 2: 99.9 percent / NaBH4; NaOH / aq. methanol / 0 - 20 °C 3: 72.8 percent / PMHS; HMDSO; pTSA / methanol; CH2Cl2 / -30 - 38 °C View Scheme
参考文献
Lim, Chongsoo; Evenson, Gerald N.; Perrault, William R.; Pearlman, Bruce A.
Tetrahedron Letters, 2006 , vol. 47, # 36 p. 6417 - 6420
反应条件
1: 92.1 percent / Si(0); KF / ethane-1,2-diol; various solvent(s) / 2 h / 140 °C 2: 99.9 percent / NaBH4; NaOH / aq. methanol / 0 - 20 °C View Scheme
参考文献
Lim, Chongsoo; Evenson, Gerald N.; Perrault, William R.; Pearlman, Bruce A.
Tetrahedron Letters, 2006 , vol. 47, # 36 p. 6417 - 6420
