sodium dihydrogenphosphate; palladium 10 on activated carbon; hydrogen in water; ethyl acetate T=0 - 10°C; P=5250.53 - 7500.75 Torr; Reagent/catalyst;

1: diisopropylamine / N,N-dimethyl-formamide / 3 h / -30 - -10 °C 2: 2,6-dimethylpyridine; hydrogen; 4-methyl-morpholine; palladium 10 on activated carbon / water; ethyl acetate / 0 - 10 °C / 5250.53 - 7500.75 Torr View Scheme