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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
153824-41-0
合成路线
(共 8 条)
3878-55-5
丁二酸单甲酯
+
60-12-8
苯乙醇
→
反应条件
153824-41-0
反应条件
iron (III) acetylacetonate; sodium carbonate in n-heptane T=105°C; 8 h; Inert atmosphere; chemoselective reaction;
参考文献
Weng, Shiue-Shien; Ke, Chih-Shueh; Chen, Fong-Kuang; Lyu, You-Fu; Lin, Guan-Ying
Tetrahedron, 2011 , vol. 67, # 9 p. 1640 - 1648
108-30-5
丁二酸酐
+
60-12-8
苯乙醇
→
反应条件
153824-41-0
反应条件
Zn(ClO4)2 in diethyl ether 5 h; Heating;
参考文献
Bartoli, Giuseppe; Bosco, Marcella; Dalpozzo, Renato; Marcantoni, Enrico; Massaccesi, Massimo; Sambri, Letizia
European Journal of Organic Chemistry, 2003 , # 23 p. 4611 - 4617
152035-97-7
→
反应条件
153824-41-0
反应条件
hydrogen; palladium in 1,4-dioxane 4 h;
参考文献
Kita, Yasuyuki; Maeda, Hiroshi; Takahashi, Fumie; Fukui, Seiji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 21 p. 2639 - 2650
153839-37-3
→
反应条件
153824-41-0
反应条件
tetrabutyl ammonium fluoride in N,N-dimethyl-formamide 1.5 h; Ambient temperature;
参考文献
Kita, Yasuyuki; Maeda, Hiroshi; Takahashi, Fumie; Fukui, Seiji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 21 p. 2639 - 2650
93790-78-4
→
反应条件
153824-41-0
反应条件
1: 45 percent / Hg(OAc)2, BF3*Et2O 2: 75 percent / p-TsOH / CH2Cl2 / 12 h / 40 °C 3: 80 percent / tetrabutylammonium fluoride / dimethylformamide / 1.5 h / Ambient temperature View Scheme
参考文献
Kita, Yasuyuki; Maeda, Hiroshi; Takahashi, Fumie; Fukui, Seiji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 21 p. 2639 - 2650
148114-03-8
→
反应条件
153824-41-0
反应条件
1: 75 percent / p-TsOH / CH2Cl2 / 12 h / 40 °C 2: 80 percent / tetrabutylammonium fluoride / dimethylformamide / 1.5 h / Ambient temperature View Scheme
参考文献
Kita, Yasuyuki; Maeda, Hiroshi; Takahashi, Fumie; Fukui, Seiji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 21 p. 2639 - 2650
153824-41-0
→
反应条件
110-15-6
琥珀酸
+
60-12-8
苯乙醇
反应条件
in water T=25°C; other temperature, ΔH(excit.), ΔS(excit.); KineticsRate constant;
参考文献
Saramma, K.; Thankamma, A.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1980 , vol. 19, # 9 p. 904 - 905
153824-41-0
→
反应条件
110-15-6
琥珀酸
+
60-12-8
苯乙醇
反应条件
in water T=25°C; other temperature, ΔH(excit.), ΔS(excit.); KineticsRate constant;
参考文献
Saramma, K.; Thankamma, A.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1980 , vol. 19, # 9 p. 904 - 905