(3R,4S,5R)-3,4-二羟基-5-(羟基甲基)二氢-2(3H)-呋喃酮合成路线 (共 17 条)
反应条件
bromine; barium carbonate in water T=0 - 20°C; Oxidation; 4.3 h;
参考文献
Bouchez, Veronique; Stasik, Imane; Beaupere, Daniel; Uzan, Raoul
Carbohydrate Research, 1997 , vol. 300, # 2 p. 139 - 142
反应条件
bromine; sodium hydrogencarbonate in water T=0 - 20°C; 4 h;
参考文献
Falentin, Celine; Beaupere, Daniel; Demailly, Gilles; Stasik, Imane
Tetrahedron, 2008 , vol. 64, # 42 p. 9989 - 9991
反应条件
potassium hydroxide in isopropyl alcohol
参考文献
G. D. Searle and Co.
Patent: US4910310 A1, 1990 ;
反应条件
hydrogenchloride; nitrogen oxides
参考文献
Thompson; Wolfrom
Journal of the American Chemical Society, 1946 , vol. 68, p. 1509
反应条件
hydrogenchloride; methanesulfonic acid in water; acetone T=20°C; 20 h;
参考文献
Fan, Ao; Jaenicke, Stephan; Chuah, Gaik-Khuan
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7720 - 7726
反应条件
water durch Eindampfen;
参考文献
Wohl; List
Chemische Berichte, 1897 , vol. 30, p. 3107
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Fischer,E.; Bromberg
Chemische Berichte, 1896 , vol. 29, p. 583
反应条件
anhydrous sodium borate; water
参考文献
Gorin; Perlin
Canadian Journal of Chemistry, 1956 , vol. 34, p. 693,699
反应条件
hydrogenchloride 1.) alkaline solution, Humphlett procedure for oxygenation , 2.) i-PrOH; Multistep reaction;
参考文献
Fleet, George W.J.; Petursson, Sigthor; Campbell, Arthur L.; Mueller, Richard A.; Behling, James R.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 665 - 666
反应条件
1: lead (IV)-acetate; acetic acid / Behandeln des Reaktionsprodukts mit Wasser in Gegenwart eines sauren Kationen-Austauschers. 2: sodium borate; water View Scheme
参考文献
Gorin; Perlin
Canadian Journal of Chemistry, 1956 , vol. 34, p. 693,699
反应条件
anhydrous sodium borate; water; acetic acid
参考文献
Isbell et al.
Journal of Research of the National Bureau of Standards (United States), 1954 , vol. 53, p. 325