4-(2-氨基-4-噻唑)-1,2-苯二醇合成路线 （共 8 条）
反应条件
in ethanol 2 h; RefluxInert atmosphere;
参考文献
Wang, Wen-Long; Chai, Sergio C.; Huang, Min; He, Hong-Zhen; Hurley, Thomas D.; Ye, Qi-Zhuang
Journal of Medicinal Chemistry, 2008 , vol. 51, # 19 p. 6110 - 6120
反应条件
AlCl3, aluminium chloride in benzene 10 h; Reflux;
参考文献
Huang, Wei-Bin; Guo, Ying; Jiang, Jian-An; Pan, Xian-Dao; Liao, Dao-Hua; Ji, Ya-Fei
Synlett, 2013 , vol. 24, # 6 art. no. ST-2013-W0052-L, p. 741 - 746
反应条件
1: phosphorus oxychloride 2: alcohol View Scheme
参考文献
Huang, Wei-Bin; Guo, Ying; Jiang, Jian-An; Pan, Xian-Dao; Liao, Dao-Hua; Ji, Ya-Fei
Synlett, 2013 , vol. 24, # 6 art. no. ST-2013-W0052-L, p. 741 - 746
反应条件
1: bromine / ethanol / 1 h / 20 °C 2: ethanol / 2 h / |Reflux 3: AlCl3, aluminium chloride / benzene / 10 h / |Reflux View Scheme
参考文献
Huang, Wei-Bin; Guo, Ying; Jiang, Jian-An; Pan, Xian-Dao; Liao, Dao-Hua; Ji, Ya-Fei
Synlett, 2013 , vol. 24, # 6 art. no. ST-2013-W0052-L, p. 741 - 746
反应条件
1: zinc(II) chloride / dichloromethane / 20 °C 2: bromine / ethanol / 1 h / 20 °C 3: ethanol / 2 h / |Reflux 4: AlCl3, aluminium chloride / benzene / 10 h / |Reflux View Scheme
参考文献
Huang, Wei-Bin; Guo, Ying; Jiang, Jian-An; Pan, Xian-Dao; Liao, Dao-Hua; Ji, Ya-Fei
Synlett, 2013 , vol. 24, # 6 art. no. ST-2013-W0052-L, p. 741 - 746
反应条件
1: potassium carbonate / ethanol / 5 h / |Reflux 2: bromine / ethanol / 1 h / 20 °C 3: ethanol / 2 h / |Reflux 4: AlCl3, aluminium chloride / benzene / 10 h / |Reflux View Scheme
参考文献
Huang, Wei-Bin; Guo, Ying; Jiang, Jian-An; Pan, Xian-Dao; Liao, Dao-Hua; Ji, Ya-Fei
Synlett, 2013 , vol. 24, # 6 art. no. ST-2013-W0052-L, p. 741 - 746
参考文献
Horii
Yakugaku Zasshi, 1935 , vol. 55, p. 14,20;dtsch.Ref.S.4
Chem.Abstr., 1935 , p. 3317
参考文献
Horii
Yakugaku Zasshi, 1935 , vol. 55, p. 14,20;dtsch.Ref.S.4
Chem.Abstr., 1935 , p. 3317
