1,2,3,5-四苯甲酰氧基-2-C-甲基-beta-D-呋喃核糖合成路线 （共 9 条）
反应条件
triethylamine in acetonitrile T=20 - 60°C; 2 - 4 h;
参考文献
Tamerlani, Giancarlo; Salsini, Liana; Lombardi, Ilaria; Bartalucci, Debora; Cipolletti, Giovanni
Patent: US2004/158059 A1, 2004 ;
Location in patent: Page 7; 9 ;
反应条件
triethylamine in acetonitrile T=60°C; 2 - 4 h;
参考文献
INALCO S.P.A.
Patent: WO2004/69851 A1, 2004 ;
Location in patent: Page 16-17; 22 ;
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane 3 h; Ambient temperature; Yields of byproduct given;
参考文献
Harry-O'kuru; Smith; Wolfe
Journal of Organic Chemistry, 1997 , vol. 62, # 6 p. 1754 - 1759
参考文献
Bio, Matthew M.; Xu, Feng; Waters, Marjorie; Williams, J. Michael; Savary, Kimberly A.; Cowden, Cameron J.; Yang, Chunhua; Buck, Elizabeth; Song, Zhiguo J.; Tschaen, David M.; Volante; Reamer, Robert A.; Grabowski, Edward J. J.
Journal of Organic Chemistry, 2004 , vol. 69, # 19 p. 6257 - 6266
反应条件
1: 83 percent / DBU, Me3SiOTf / acetonitrile / 4 h / 60 °C 2: 72 percent / methanolic NH3 / 7 h / Ambient temperature View Scheme
参考文献
Franchetti, Palmarisa; Cappellacci, Loredana; Marchetti, Stefano; Trincavelli, Letizia; Martini, Claudia; Mazzoni, Maria R.; Lucacchini, Antonio; Grifantini, Mario
Journal of Medicinal Chemistry, 1998 , vol. 41, # 10 p. 1708 - 1715
反应条件
1: 57 percent / N,O-bis(trimethylsilyl)acetamide, SnCl4 / acetonitrile / 3 h / Heating 2: 87 percent / ammonia gas / methanol / 48 h View Scheme
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
反应条件
N,O-bis-(trimethylsilyl)-acetamide; ammonia; tin(IV) chloride 1.) acetonitrile, reflux, 3 h; 2.) MeOH; Multistep reaction;
参考文献
Wolfe; Harry-O'kuru
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7611 - 7614
反应条件
1: TMSOTf; BSA / acetonitrile / 3 h / 60 °C 2: ethanol / 4 h / 50 °C View Scheme
参考文献
Harry-O'kuru, Rogers E.; Kryjak, Emily A.; Wolfe, Michael S.
Nucleosides and Nucleotides, 1997 , vol. 16, # 7-9 p. 1457 - 1460
反应条件
N,O-bis-(trimethylsilyl)-acetamide; ammonia; tin(IV) chloride 1.) acetonitrile, reflux, 3 h; 2.) MeOH; Multistep reaction;
参考文献
Wolfe; Harry-O'kuru
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7611 - 7614
