3-异丙基-2,4-戊二酮合成路线 （共 15 条）
反应条件
P(MeNCH2CH2)3N in hexane; acetonitrile T=25°C; 0.5 h;
参考文献
Arumugam, Subramaniam; McLeod, Dale; Verkade, John G.
Journal of Organic Chemistry, 1998 , vol. 63, # 11 p. 3677 - 3679
反应条件
zinc(II) chloride T=110°C; bei anschliessenden Behandeln mit Wasser;
参考文献
Mao,C.-L. et al.
Journal of Organic Chemistry, 1969 , vol. 34, # 5 p. 1425 - 1429
反应条件
C34H33NP2Pt(2+)*2F6Sb(1+) in CD3NO2 T=70°C; P=1500.15 Torr; 24 h; Autoclave;
参考文献
Cucciolito, Maria E.; Damora, Angela; Vitagliano, Aldo
Organometallics, 2010 , vol. 29, # 22 p. 5878 - 5884
反应条件
boron trifluoride beim Erhitzen des Reaktionsgemisches mit wss. Natriumacetat-Loesung;
参考文献
Young et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 3635,3639, 3642
反应条件
in diethyl ether T=0°C; 2 h;
参考文献
Pedersen, Uffe; Rasmussen, Preben B.; Lawesson, Sven-Olov
Liebigs Annalen der Chemie, 1985 , # 8 p. 1557 - 1569
反应条件
1: sulfoacetic acid / 60 - 80 °C 2: boron fluoride / beim Erhitzen des Reaktionsgemisches mit wss. Natriumacetat-Loesung View Scheme
参考文献
Young et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 3635,3639, 3642
反应条件
sodium hydroxide; sodium tetrahydroborate in ethanol
参考文献
Ichikawa,K. et al.
Journal of Organic Chemistry, 1966 , vol. 31, p. 447 - 452
反应条件
N(Et)4(1+)*(2-pyrrolidone-anion) 1.) DMF, RT, 15 min, 2.) RT, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Shono, Tatsuya; Kashimura, Shigenori; Sawamura, Masaya; Soejima, Takeshi
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 907 - 910
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Kurts,A.L. et al.
Tetrahedron, 1971 , vol. 27, p. 4777 - 4785
参考文献
Hooz,J.; Smith,J.
Journal of Organic Chemistry, 1972 , vol. 37, p. 4200 - 4202
