N-乙酰基-2-甲基-1-丙胺合成路线 （共 34 条）
反应条件
methanecarbohydroxamic acid; sulfuric acid in acetonitrile T=80°C; P=1292.9 Torr; 0.166667 h; Microwave irradiation;
参考文献
Madabhushi, Sridhar; Chinthala, Narsaiah; Vangipuram, Venkata Sairam; Godala, Kondal Reddy; Jillella, Raveendra; Mallu, Kishore Kumar Reddy; Beeram, China Ramanaiah
Tetrahedron Letters, 2011 , vol. 52, # 46 p. 6103 - 6107
反应条件
methanecarbohydroxamic acid; sulfuric acid in acetonitrile 11.5 h; Reflux;
参考文献
Madabhushi, Sridhar; Chinthala, Narsaiah; Vangipuram, Venkata Sairam; Godala, Kondal Reddy; Jillella, Raveendra; Mallu, Kishore Kumar Reddy; Beeram, China Ramanaiah
Tetrahedron Letters, 2011 , vol. 52, # 46 p. 6103 - 6107
反应条件
triethylamine in dichloromethane T=20°C; Acetylation; 0.583333 h;
参考文献
Whitehouse, Darren L.; Nelson Jr., Kingsley H.; Savinov, Sergey N.; Loewe, Ralf S.; Austin, David J.
Bioorganic and Medicinal Chemistry, 1998 , vol. 6, # 8 p. 1273 - 1282
反应条件
ammonia in acetonitrile byproducts: trans-2-butene, cis-2-butene; i-BuSnMe3 in CH3CN added to Fe(phen)3(PF6)3 in CH3CN at 22°C under Ar and soln. stirred for 2 h, drop water added and Fe(II) complex filtered, filtrate dried with MgSO4 and treated anhyd. NH3 and Sn product filtered;
参考文献
Rollick; Kochi
Journal of the American Chemical Society, 1982 , vol. 104, # 5 p. 1319 - 1330
反应条件
iron(III) chloride T=90°C; Beckmann rearrangement of ketoximes; 2 h;
参考文献
Khodaei; Meybodi; Rezai; Salehi
Synthetic Communications, 2001 , vol. 31, # 13 p. 2047 - 2050
反应条件
tetrabutylammonium (meta)periodate in dichloromethane Ambient temperature;
参考文献
Atkinson, Robert N.; Storey, Bernadette M.; King, S. Bruce
Tetrahedron Letters, 1996 , vol. 37, # 52 p. 9287 - 9290
反应条件
in benzene T=15°C; Yang cyclization; 5 h; UV-irradiation;
参考文献
Griesbeck, Axel G.; Heckroth, Heike
Journal of the American Chemical Society, 2002 , vol. 124, # 3 p. 396 - 403
参考文献
Lock,M.V.; Sagar,B.F.
Journal of the Chemical Society [Section] B: Physical Organic, 1966 , p. 690 - 696
反应条件
sodium hydroxide 1.) acetonitrile, 22 deg C; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Rollick; Kochi
Journal of the American Chemical Society, 1982 , vol. 104, # 5 p. 1319 - 1330
反应条件
in benzene 4 h; Heating;
参考文献
Morita; Tsuda; Kise; Sugiyama
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 3 p. 1139 - 1142
