trichlorophosphate T=115°C; 48 h;

1: 94 percent / H2 / Raney-nickel / tetrahydrofuran / 21 h / 26 - 34 °C / 1241.2 - 2585.7 Torr 2: 91 percent / hexafluorophosphoric acid, aq. NaNO2 / 0.08 h 3: 27 percent / 150 °C 4: 97 percent / 1.0 N aq. NaOH / tetrahydrofuran / 0.5 h / 5 - 20 °C View Scheme

1: 94 percent / H2 / Raney-nickel / tetrahydrofuran / 21 h / 26 - 34 °C / 1241.2 - 2585.7 Torr 2: 91 percent / hexafluorophosphoric acid, aq. NaNO2 / 0.08 h 3: 27 percent / 150 °C View Scheme

hydrogen; nickel in tetrahydrofuran T=26 - 34°C; P=1241.2 - 2585.7 Torr; 21 h;

ammonia; triethylamine in 1,4-dioxane; dichloromethane T=0°C;