3-(溴甲基)-5-苯基异噁唑合成路线 （共 4 条）
反应条件
PPh3.Br2 in dichloromethane 1 h; Ambient temperature;
参考文献
Pei; Wickhan
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7509 - 7512
反应条件
1: 95 percent / LiAlH4 / tetrahydrofuran / 0.5 h / -78 °C 2: 97 percent / Ph3PBr2 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Pei; Wickhan
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7509 - 7512
反应条件
1: 100 percent / NH2OH*HCl / ethanol / 2 h / Heating 2: 95 percent / LiAlH4 / tetrahydrofuran / 0.5 h / -78 °C 3: 97 percent / Ph3PBr2 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Pei; Wickhan
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7509 - 7512
反应条件
1: 99 percent / NaH / toluene / 1 h / Heating 2: 100 percent / NH2OH*HCl / ethanol / 2 h / Heating 3: 95 percent / LiAlH4 / tetrahydrofuran / 0.5 h / -78 °C 4: 97 percent / Ph3PBr2 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Pei; Wickhan
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7509 - 7512
