3-溴-5-(n-boc)氨基甲基异噁唑合成路线 (共 4 条)
反应条件
triethylamine in dichloromethane T=0 - 20°C; 72.4167 h;
参考文献
WO2007/61763 A2, ;
Page/Page column 33 ;
WO 2007/061763 A2
反应条件
diphenyl phosphoryl azide; triethylamine 13.5 h; Heating / reflux;
参考文献
COMENTIS, INC.; BILCER, Geoffrey, M.; LILLY, John, C.; SWANSON, Lisa, M.
Patent: WO2011/130383 A1, 2011 ;
Location in patent: Page/Page column 80 ;
WO 2011/130383 A1
反应条件
TEA; phenyl isocyanate
参考文献
Pei; Wickhan
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7509 - 7512
反应条件
trifluoroacetic acid in dichloromethane
参考文献
Pei; Wickhan
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7509 - 7512