反应条件
1.1: magnesium / tetrahydrofuran / 0.75 h / Heating 1.2: tetrahydrofuran / -16 - -14 °C 1.3: tetrahydrofuran / 1 h 2.1: 0.176 g / 0.25 h 3.1: triethyl amine / CH2Cl2 / 3 h / 20 °C 4.1: 0.110 g / DBU / 12 h / 60 °C 5.1: hydrogen / palladium on charcoal / methanol / 8 h / 65 °C / 10343 Torr 6.1: 0.041 g / HBr / 5 h / Heating View Scheme
参考文献
Chavan, Subhash P.; Ramakrishna, Guduru; Gonnade, Rajesh G.; Bhadbhade, Mohan M.
Tetrahedron Letters, 2004 , vol. 45, # 39 p. 7307 - 7310
